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测量应用案例-20191110

2019-11-23 13:53:59

1107

文献名:ZrS3: From crystalline samples to colloid dispersions 

 

上海弘升科技發展有限公司Pavel Poltaraka, Anastasiia Poltaraka, Sofya Artemkinaab, Tatyana Podlipskayab, Igor Asanovb, Vladimir Fedorovab 

aNovosibirsk State University, 2, Pirogova Str., 630090 Novosibirsk, Russian Federation

bNikolaev Institute of Inorganic Chemistry SB RAS, 3, Akad. Lavrentiev Ave., 630090 Novosibirsk, Russian Federation

 

摘要:A series of ZrS3 samples have been synthesized from elements at temperatures from 350 to 650°C. Stable ZrS3 colloid dispersions in different organic media (acetonitrile, dimethylformamide, ethanol, and isopropanol) were obtained from the polycrystalline samples. The structural and spectroscopic identities of the ZrS3 particles were confirmed by X-ray powder diffraction and Raman spectra. The sizes and morphology of particles in the colloid dispersions have been studied by transmission electron microscopy and dynamic light scattering method; the concentrations of the dispersions were found to depend on condition of synthesis of the initial bulk ZrS3.


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